@article{oai:shiga-u.repo.nii.ac.jp:00001736,
 author = {糸乗, 前 and 高橋, 将人 and 木村, 幸史 and 杉田, 陸海},
 issue = {51},
 journal = {滋賀大学教育学部紀要, 3, 自然科学},
 month = {},
 note = {Departmental Bulletin Paper, The　stability　of　the　C-P　bond　to　hydrolysis　provides　a　basis　for　differential　estimation　of　C-P  compounds　in　the　presence　of　C-O-P　compounds.　The　C-P　bond　is　not　degraded　by　strong　mineral  acids　or　alkalis　but　is　degraded　by　digestion　with　perchloric　acid.　The　difference　between　the  total　phosphorous,　measured　after　perchloric　acid　digestion,　and　phosphate　phosphorous(C-O-P bond-type　phosphorous) liberated　by　acid　hydrolysis　represents　the　amount　of　C-P　phosphorous
[Pc-p ＝P total -Phydrolyzable].　To  determine  Phydrolyzable,　it　is  necessary　to　hydrolyze　by  strong　mineral  acids  for  long　times.  The　conventional　method　requires　reaction　for  40　hours  or　longer　in　a　boiling　water　bath　or　heating　oven,　which　is　a　time-consuming　step.  Recently,　several　reaction　times　have　been　reduced　using　a　microwave　oven.　Here,　we　describe  a  method　for　applying　microwave-mediated　reaction　to　phosphorous　analysis.　By　the　microwave  method,　the　hydrolysis　of　C-O-P　bond　is　rapid　and　complete　with　only　1　minute　and　50　seconds  exposure., 滋賀大学教育学部紀要, 3, 自然科学, 第51号, pp.1-5},
 pages = {1--5},
 title = {電磁波分解におけるC-O-PおよびC-P結合の安定性},
 year = {2001}
}